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林业科学 ›› 2013, Vol. 49 ›› Issue (11): 135-140.doi: 10.11707/j.1001-7488.20131119

• 论文与研究报告 • 上一篇    下一篇

麻竹竹叶的化学成分

王淑英, 岳永德, 汤锋, 孙嘏, 魏琦, 喻谨   

  1. 国际竹藤中心 北京 100102
  • 收稿日期:2012-12-21 修回日期:2013-01-24 出版日期:2013-11-25 发布日期:2013-11-26
  • 通讯作者: 岳永德
  • 基金资助:

    国家科技支撑计划项目(2012BAD23B03)。

Chemical Constituents from the Leaves of Dendrocalamus latiflorus

Wang Shuying, Yue Yongde, Tang Feng, Sun Jia, Wei Qi, Yu Jin   

  1. International Center for Bamboo and Rattan Beijing 100102
  • Received:2012-12-21 Revised:2013-01-24 Online:2013-11-25 Published:2013-11-26

摘要:

采用硅胶柱色谱、Sephadex LH-20柱色谱、高压制备色谱及重结晶等方法从麻竹叶乙醇提取物中分离得到15个化合物,根据理化性质和光谱数据,分别鉴定为木犀草素、苜蓿素、7-甲氧基-苜蓿素、苜蓿素-4’-O-葡萄糖苷、苜蓿素-7-O-葡萄糖苷、芹菜素、芹菜素-7-O-葡萄糖苷、芹菜素-6-C-阿拉伯糖苷、芹菜素-7-O-葡萄糖-6″-O-鼠李糖苷、对羟基苯甲醛、5-羟基-2-甲氧基-苯甲醛、黑麦草内酯、去氢催吐萝芙木醇、催吐萝芙木醇-9-O-葡萄糖苷和4,4’,9,9’-四羟基-3,3’,5,5’-四甲氧基-7,7’-单环氧木脂素。研究结果为麻竹叶资源的开发利用提供科学依据,为阐明麻竹叶药理活性奠定基础。

关键词: 麻竹, 竹叶, 化学成分, 结构鉴定

Abstract:

To study the chemical constituents from the leaves of Dendrocalamus latiflorus, the compounds were isolated by column chromatography on silica gel, Sephadex LH-20, Prep HPLC and recrystallization. Their structures were elucidated on the basis of physicochemical constants and spectral analysis. Fifteen compounds were isolated and identified as luteolin, tricin, 7-methoxy-tricin, tricin-4'-O-glucopyranoside, tricin-7-O-glucopyranoside, apigenin, apigenin-7-O-glucopyranoside, apigenin-6-C-arabinfuranoside, apigenin-7-O-glucopyranoside-6"-O-rhamnoside, p-hydroxybenzaldehyde, 5-hydroxy-2-methoxy-benzaldehyde, loliolide, dehydrovomifoliol, vomifoliol-9-O-glucopyranoside, 4,4',9,9'-tetrahydroxy-3,3',5,5'-tetramethoxy-7,7'-monoepoxy lignan. The results of the research provided scientific basis for development and utilization of bamboo leaves. It established the foundation for clarification pharmacological activity of the leaves of Dendrocalamus latiflorus.

Key words: Dendrocalamus latiflorus, bamboo leaves, chemical constituents, structural identification

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